A.S.T.M DISTILLATION

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An A.S.T.M. distillation is a simple distillation using The equipment consists of Borosilicate glass round bottom flask as distillation still . The distillation is carried out by heating the still. The vapors coming from the column is going in to the condenser. The distillate is collected in measuring flask.

RANGE OF EXPERIMENTS TO BE CARRIED OUT : 

To A.S.T.M. Distillation

EXPERIMENTAL SETUP :

Reboiler                       :           Borosilicate glass round bottom flask

Distillate Receiver       :           Borosilicate glass measuring cylinder

Condenser                  :           Borosilicate glass double pipe condenser

Heating Mantle            :           Aluminum body with fiber cloth and

with Thermostat

Digital Temp Indicator :           0 – 400 0 C .

Temp Sensor              :           CR/AL

Type Piping                :           PVC

Setup Mounting           :           On sturdy MS stand with

powder coated

SPACE REQUIRED             :           1.5 m. (L) x 1.0 m(W) X 2 m (H) 

SERVICE REQUIRED           :           Power  Supply   : 230 V, 50 Hz, A. C.

CHEMICALS REQUIRED     :           Methanol Or Ethanol

WEIGHT                                 :           @ 45 Kg

DIFFUSION CO-EFFICIENT OF CCL- 4 IN AIR SALT IN WATER

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The experimental set up consists of glass U tube with a capillary base. The U tube is immersed in water tank.  In order to carry out diffusion at different temperatures,   water is circulated by means of pump through a geyser.  A scale is provided in front of the capillary for measurement of fall liquid level.  Fan is provided to blow a gentle current of air over the capillary box, at a rate controlled by a valve. The tank temperature & in turn the liquid temperature is measured by the thermometer         

RANGE OF EXPERIMENTS TO BE CARRIED OUT :

Study of diffusion of CCL4 in air

To estimate the diffusivity of vapor in air

EXPERIMENTAL SETUP :

Stephens Tube                        :           Borosilicate Glass

Water Supply Tank                 :           Material Mild Steel

Heater                                     :           Nichrome Wire

Pump                                      :           FHP Pump

Pump                                      :           Compactable Capacity

Measuring Scale                     :           1No.

Thermostat                              :           1 No.

Digital Temp Indicator            :            0 – 200 0 C ., Indicator cum Controller Temp

Sensor                                     :           CR/AL

Type Piping                             :           SS , PVC

Setup Mounting                       :           On sturdy MS stand with

powder coated

SPACE REQUIRED             :           1.0 m. (L) x 1.0 m(W) X 1.0 m (H) 

SERVICE REQUIRED           :           Power  Supply   : 230 V, 50 Hz, A. C.

CHEMICALS REQUIRED     :           CCL4

WEIGHT                                 :           @ 45 Kg

SINGLE DROP EXTRACTION COLUMN

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An experimental setup Consist of glass column in which single drop extraction is carried out.

RANGE OF EXPERIMENTS TO BE CARRIED OUT :

To determine overall mass transfer co-efficient based on

continuous and dispersed phase.

To determine individual Height of Transfer Unit based on

continuous and dispersed phase.

To determine Overall Number of Transfer Unit based on

continuous and dispersed phase.

EXPERIMENTAL SETUP : 

Column                                   :           Borosilicate Glass Column

Feed Tank                               :           1 No. of stainless steel feed tank

Piping                                      :           SS , PVC

Setup Mounting                       :           On sturdy MS stand with

powder coated 

SPACE REQUIRED              :          1.5 m. (L) x 1.0 m(W) X 2.0 m (H)

SERVICE REQUIRED           :           Air Supply :      : @ 6 CFM, at4 Kg /cm2. 

CHEMICALS REQUIRED     :           Tolune , Acetic Acid , Distilled Water

, NaOH , Phenolphthalein , Benzene

WEIGHT                                 :           @ 65 Kg

YORK – SCHEIBEL COLUMN

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The York Scheibel’s column falls in the class of gravity – operated extractors with mechanical agitation. The presence of alternatively agitating and calming sections in York Scheibel’s column yield higher extraction efficiency than the conventional packed column. Each stage consist of a woven wire mesh section and mixing section. The total set – up is housed in a well designed rigid structure. The structure also supports tanks, piping, Rota meter ,piping and other units.

RANGE OF EXPERIMENTS TO BE CARRIED OUT :

To determine overall mass transfer co-efficient based on continuous and dispersed phase.

To determine individual Height of Transfer Unit based on continuous and dispersed phase.

To determine Overall Number of Transfer Unit based on continuous and dispersed phase.

EXPERIMENTAL SETUP :

Column                       :           Borosilicate Glass Column

Packing                       :           Stainless Steel Woven Mesh

Agitator                        :           Variable Speed Agitator

Digital RPM Indicator :            0 -999 RPM

Flow Measurement     :           2 No. Pre calibrated Rota meter

Feed Tank                   :           2 No. of stainless steel feed tank

Extract Receiver         :           1 No. of stainless steel tank

Raffinate Receiver     :           1 No. of stainless steel tank

Feed Circulation          :           By Compressed Air

Pressure Regulator     :           0 – 2 kgf / cm2

Pressure Gauge          :           Bourdon type 0 – 2 kgf / cm2

Piping                          :           SS , PVC

Setup Mounting           :           On sturdy MS stand with

powder coated

SPACE REQUIRED  :          1.5 m. (L) x 1.0 m(W) X 1.5 m (H)

SERVICE REQUIRED :         Air Supply :      : @ 6 CFM, at 4 Kg /cm2. 

CHEMICALS REQUIRED :   Tolune , Acetic Acid , Distilled Water

, NaOH , Phenolphthalein , Benzene

WEIGHT                            :    @ 65 Kg

PACKED COLUMN EXTRACTION

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The set up consists of a Borosilicate glass column provided with rasching rings packing. The column is provided with liquid distributor at the bottom & top. Overhead Feed tanks are provided with arrangement to arrange the flow rates through calibrated Rota meter.

RANGE OF EXPERIMENTS TO BE CARRIED OUT :

To calculate the Number of transfer unit.

To calculate the Overall height of transfer unit.

To calculate the overall volumetric mass transfer coefficient.

EXPERIMENTAL SETUP :

Column                       :           Borosilicate Glass Column

Packing                       :           Rasching Ring

Flow Measurement     :           2 No. Pre calibrated Rota meter

Feed Tank                   :           2 No. of stainless steel feed tank

Extract Receiver         :           1 No. of stainless steel tank

Raffinate Receiver     :           1 No. of stainless steel tank

Feed Circulation          :           By Compressed Air

Pressure Regulator     :           0 – 2 kgf / cm2

Pressure Gauge          :           Bourdon type 0 – 2 kgf / cm2

Piping                          :           SS , PVC

Setup Mounting           :           On sturdy MS stand with

powder coated

SPACE REQUIRED  :          1.5 m. (L) x 1.0 m(W) X 1.5 m (H)

SERVICE REQUIRED :         Air Supply :      : @ 6 CFM, at 4 Kg /cm2. 

CHEMICALS REQUIRED :   Tolune , Acetic Acid , Distilled Water

, NaOH , Phenolphthalein , Benzene 

WEIGHT                            :    @ 65 Kg

LIQUID – LIQUID EXTRACTION (SPRAY COLUMN)

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An experimental setup of liquid liquid extractor having counter current flow pattern of solvent and solute to get extract and raffinate streams. The flowmeter will be provided for measuring flow rates of solute and solvent. The continuous and disperse phases will be derived in separate containers

RANGE OF EXPERIMENTS TO BE CARRIED OUT : 

To calculate the Number of transfer unit.

To calculate the Overall height of transfer unit.

To calculate the overall volumetric mass transfer coefficient.

EXPERIMENTAL SETUP : 

Column                       :           Borosilicate Glass Column

Flow Measurement     :           2 No. Pre calibrated Rota meter

Feed Tank                   :           2 No. of stainless steel feed tank

Extract Receiver         :           1 No. of stainless steel tank

Raffinate Receive       :           1 No. of stainless steel tank

Feed Circulation          :           By Compressed Air

Pressure Regulator     :           0 – 2 kgf / cm2

Pressure Gauge          :           Bourdon type 0 – 2 kgf / cm2

Piping                          :           SS , PVC

Setup Mounting           :           On sturdy MS stand with

powder coated

SPACE REQUIRED  :          1.5 m. (L) x 1.0 m(W) X 1.5 m (H)

SERVICE REQUIRED :         Air Supply :      : @ 6 CFM, at 4 Kg /cm2. 

CHEMICALS REQUIRED :   Tolune , Acetic Acid , Distilled Water

, NaOH , Phenolphthalein , Benzene 

WEIGHT                            :    @ 65 Kg

BATCH DISTILLATION

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The unit consists of a packed column with rasching rings. Two necked round bottom borosilicate glass flask with a heating metal is used as a reboiler. The vapor stream flows up the column & is condensed in the condenser. The flow rate of cooling water can be measured through Rota meter & that of the reflux by the Rota meter. The temperature of various streams can be measured.

RANGE OF EXPERIMENTS TO BE CARRIED OUT :

To carryout Batch distillation.

To study the practical significance of McCabe – Thiele method.

EXPERIMENTAL SETUP :

Reboiler                       :           Material Stainless Steel

Column                       :           Material Stainless Steel

Reflux Drum               :           Material Stainless Steel

Condenser                  :           SS , Shell and

Tube type Condenser

Flow Measurement     :           2 No. Pre calibrated Rota meter

Packing                       :           Rasching Ring.

Heating Mantle            :           Aluminum body with fiber cloth

Digital Temp Indicator :           0 – 400 0 C.

Temp Sensor              :           CR/AL Type

Distillate Receiver       :           Material Stainless Steel

Piping                          :           SS , PVC

Setup Mounting           :           On sturdy MS stand with

powder coated

SPACE REQUIRED :           1.5 m. (L) x 1.0 m(W) X 3 m (H)

SERVICE REQUIRED:          Power Supply : 230 V, 50 Hz, A.C.

Water Supply              :           @ 2 lpm

Specific Gravity Bottle

CHEMICALS REQUIRED :   Methanol Or Ethanol

WEIGHT                           :     @ 65 Kg

PACKED COLUMN DISTILLATION

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The unit consists of a packed column with rasching rings. Two necked round bottom borosilicate glass flask with a heating metal is used as a reboiler. The vapor stream flows up the column & is condensed in the condenser. The flow rate of cooling water can be measured through Rota meter & that of the reflux by the Rota meter. The temperature of various stream can be measured.

RANGE OF EXPERIMENTS TO BE CARRIED OUT : 

To carryout Packed column distillation.

To study the practical significance of McCabe – Thiele method.

EXPERIMENTAL SETUP : 

Reboiler                                   :           Material Stainless Steel OR

Borosilicate Glass Column     :           Material Stainless Steel ,OR

Borosilicate Glass Condenser SS ,

Shell and Tube type Condenser ,OR

Double pipe , Borosilicate glass

Flow Measurement                 :           2 No. Pre calibrated Rota meter

Packing                                   :           Rasching Ring.

Heating Mantle                        :           Aluminum body with fiber cloth

Digital Temp Indicator             :           0 – 400 0 C .

Temp Sensor                          :           CR/AL Type

Distillate Receiver                   :           Material Stainless Steel OR

Borosilicate Glass

Piping                                     :           SS , PVC

Setup Mounting                       :           On sturdy MS stand with

powder coated

SPACE REQUIRED                          :           1.5 m. ( L) x 1.0 m (W) X 3 m (H).

SERVICE REQUIRED           :           Power Supply : 230 V, 50 Hz, A.C.

Water Supply : @ 2 lpm

Specific Gravity Bottle

CHEMICALS REQUIRED     :           Methanol Or Ethanol

WEIGHT                                 :           @ 65 Kg

FRACTIONAL DISTILLATION COLUMN GLASS

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RANGE OF EXPERIMENTS TO BE CARRIED OUT:

  1. To carryout Fractional distillation.

EXPERIMENTAL SETUP : 

Reboiler                       :           Borosilicate glass

Column                       :           Borosilicate glass

Condenser                  :           Borosilicate glass

Packing                       :           Rascig rings

Heating Mantle            :           Aluminum body with fiber cloth

Digital Temp Indicator :           0 – 400 0 C .

Temp Sensor              :           CR/AL Type

Distillate Receiver       :           Borosilicate glass

Piping                          :           SS , PVC

Setup Mounting           :           On sturdy MS stand with

powder coated

SPACE REQUIRED :           1.5 m. (L) x 1.0 m(W) X 3 m (H)

SERVICE REQUIRED :         Power Supply : 230 V, 50 Hz, A.C.

Water Supply : @ 2 lpm

Specific Gravity Bottle

CHEMICALS REQUIRED :  Methanol Or Ethanol ,

Specific Gravity Bottle

WEIGHT :  @ 65 Kg

FRACTIONAL DISTILLATION COLUMN

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The distillation column made of SS material. An electrically heated reboiler would be installed at the bottom of the column. The vapors from the top of the column are condensed in the condenser by circulating cooling water. The condensate is collected in reflux drum and feed back to the column as reflux. The complete column is insulated

RANGE OF EXPERIMENTS TO BE CARRIED OUT:

  1. To carryout Fractional distillation.
  2. To calculate the number of trays required
  3. To establish the overall tray efficiency of the fractional distillation
  4. To study the practical significance of McCabe – Thiele method.

EXPERIMENTAL SETUP : 

Reboiler                       :           Material Stainless Steel

Column                       :           Material Stainless Steel

Condenser                  :           SS , Shell and Tube type Condenser

Reflux Drum               :           Material Stainless Steel.

Heating Mantle            :           Aluminum body with fiber cloth

Digital Temp Indicator :           0 – 400 0 C .

Temp Sensor              :           CR/AL Type

Distillate Receiver       :           Material Stainless Steel

Piping                          :           SS , PVC

Setup Mounting           :           On sturdy MS stand with

powder coated

SPACE REQUIRED :           1.5 m. (L) x 1.0 m(W) X 3 m (H)

SERVICE REQUIRED :         Power Supply : 230 V, 50 Hz, A.C.

Water Supply : @ 2 lpm

Specific Gravity Bottle

CHEMICALS REQUIRED :  Methanol Or Ethanol ,

Specific Gravity Bottle

WEIGHT :  @ 65 Kg