LIQUID LIQUID EXTRACTION ( SPRAY COLUMN )

extractor having counter current flow pattern of solvent and solute to get extract and raffinate streams. The flowmeter will be provided for measuring flow rates of solute and solvent. The continuous and disperse phases will be derived in separate containers
RANGE OF EXPERIMENTS TO BE CARRIED OUT :
To calculate the Number of transfer unit.
To calculate the Overall height of transfer unit.
To calculate the overall volumetric mass transfer coefficient.
EXPERIMENTAL SETUP :
Column : Borosilicate Glass Column
Flow Measurement : 2 No. Pre calibrated Rota meter
Feed Tank : 2 No. of stainless steel feed tank
Extract Receiver : 1 No. of stainless steel tank
Raffinate Receive : 1 No. of stainless steel tank
Feed Circulation : By Compressed Air
Pressure Regulator : 0 – 2 kgf / cm2
Pressure Gauge : Bourdon type 0 – 2 kgf / cm2
Piping : SS , PVC
Setup Mounting : On sturdy MS stand with
powder coated
SPACE REQUIRED : 1.5 m. (L) x 1.0 m(W) X 1.5 m (H)
SERVICE REQUIRED : Air Supply : : @ 6 CFM, at 4 Kg /cm2.
CHEMICALS REQUIRED : Tolune , Acetic Acid , Distilled Water
, NaOH , Phenolphthalein , Benzene
WEIGHT : @ 65 Kg

Get More Details:- 21- LIQUID LIQUID EXTRACTION SPRAY COLUMN

LIQUID LIQUID EXTRACTION ( PACKED COLUMN )

DESCRIPTION : An experimental setup of liquid liquid extractor having counter current flow pattern of solvent and solute to get extract and raffinate streams. The flowmeter will be provided for measuring flow rates of solute and solvent. The continuous and disperse phases will be derived in separate containers
RANGE OF EXPERIMENTS TO BE CARRIED OUT :
To calculate the Number of transfer unit.
To calculate the Overall height of transfer unit.
To calculate the overall volumetric mass transfer coefficient.
EXPERIMENTAL SETUP :
Column : Borosilicate Glass Column
Flow Measurement : 2 No. Pre calibrated Rota meter
Feed Tank : 2 No. of stainless steel feed tank
Extract Receiver : 1 No. of stainless steel tank
Raffinate Receive : 1 No. of stainless steel tank
Feed Circulation : By Compressed Air
Pressure Regulator : 0 – 2 kgf / cm2
Pressure Gauge : Bourdon type 0 – 2 kgf / cm2
Piping : SS , PVC
Setup Mounting : On sturdy MS stand with
powder coated
SPACE REQUIRED : 1.5 m. (L) x 1.0 m(W) X 1.5 m (H)
SERVICE REQUIRED : Air Supply : : @ 6 CFM, at 4 Kg /cm2.
CHEMICALS REQUIRED : Tolune , Acetic Acid , Distilled Water
, NaOH , Phenolphthalein , Benzene
WEIGHT : @ 65 Kg

Get More Details:- 22- LIQUID LIQUID EXTRACTION PACKED COLUMN

YORK SCHEIBEL EXTRACTION COLUMN

DESCRIPTION : The York Scheibel’s column falls in the class of gravity – operated extractors with mechanical agitation. The presence of alternatively agitating and calming sections in York Scheibel’s column yield higher extraction efficiency than the conventional packed column. Each stage consist of a woven wire mesh section and mixing section. The total set – up is housed in a well designed rigid structure. The structure also supports tanks, piping, Rota meter ,piping and other units.
RANGE OF EXPERIMENTS TO BE CARRIED OUT :
To determine overall mass transfer co-efficient based on continuous and dispersed phase.
To determine individual Height of Transfer Unit based on continuous and dispersed phase.
To determine Overall Number of Transfer Unit based on continuous and dispersed phase.

EXPERIMENTAL SETUP :
Column : Borosilicate Glass Column
Packing : Stainless Steel Woven Mesh
Agitator : Variable Speed Agitator
Digital RPM Indicator : 0 -999 RPM
Flow Measurement : 2 No. Pre calibrated Rota meter
Feed Tank : 2 No. of stainless steel feed tank
Extract Receiver : 1 No. of stainless steel tank
Raffinate Receiver : 1 No. of stainless steel tank
Feed Circulation : By Compressed Air
Pressure Regulator : 0 – 2 kgf / cm2
Pressure Gauge : Bourdon type 0 – 2 kgf / cm2
Piping : SS , PVC
Setup Mounting : On sturdy MS stand with
powder coated
SPACE REQUIRED : 1.5 m. (L) x 1.0 m(W) X 1.5 m (H)
SERVICE REQUIRED : Air Supply : : @ 6 CFM, at 4 Kg /cm2.
CHEMICALS REQUIRED : Tolune , Acetic Acid , Distilled Water
, NaOH , Phenolphthalein , Benzene
WEIGHT : @ 65 Kg

Get More Details:- 23- YORK SCHEEBEL EXTRACTION COLUMN

ROTATING DISC EXTRACTION COLUMN

DESCRIPTION : The Rotating disk contactor consist of tower which is formed by annular baffles. In the setup a continuous counter current contact between the solute and solvent faces are made which results into extract and raffinate streams. Flow meter notes the flow of solvent and solute respectively. The continuous and dispersed phases streams are metered and derived from separate streams are derived from separate containers. Each compartment agitation provided by rotating, centrally located horizontal disk
RANGE OF EXPERIMENTS TO BE CARRIED OUT :
To determine overall mass transfer co-efficient based on
continuous and dispersed phase.
To determine individual Height of Transfer Unit based on
continuous and dispersed phase.
To determine Overall Number of Transfer Unit based on
continuous and dispersed phase.

EXPERIMENTAL SETUP :
Column : Stainless Steel Column
Packing : Rotating disk
Agitator : Variable Speed Agitator
Digital RPM Indicator : 0 -999 RPM
Flow Measurement : 2 No. Pre calibrated Rota meter
Feed Tank : 2 No. of stainless steel feed tank
Extract Receiver : 1 No. of stainless steel tank
Raffinate Receiver : 1 No. of stainless steel tank
Feed Circulation : By Compressed Air
Pressure Regulator : 0 – 2 kgf / cm2
Pressure Gauge : Bourdon type 0 – 2 kgf / cm2
Piping : SS , PVC
Setup Mounting : On sturdy MS stand with
powder coated
SPACE REQUIRED : 1.5 m. (L) x 1.0 m(W) X 1.5 m (H)
SERVICE REQUIRED : Power Supply : 230 V, 50 Hz, A. C.
Air Supply : : @ 6 CFM, at4 Kg /cm2.
CHEMICALS REQUIRED : Tolune , Acetic Acid , Distilled Water
, NaOH , Phenolphthalein , Benzene
WEIGHT : @ 65 Kg

Get More Details:- 24- ROTATING DISC EXTRACTION COLUMN

SINGLE DROP EXTRACTION COLUMN

DESCRIPTION : An experimental setup Consist of glass column in which single drop extraction is carried out.
RANGE OF EXPERIMENTS TO BE CARRIED OUT :
To determine overall mass transfer co-efficient based on
continuous and dispersed phase.
To determine individual Height of Transfer Unit based on
continuous and dispersed phase.
To determine Overall Number of Transfer Unit based on
continuous and dispersed phase.
EXPERIMENTAL SETUP :
Column : Borosilicate Glass Column
Feed Tank : 1 No. of stainless steel feed tank
Piping : SS , PVC
Setup Mounting : On sturdy MS stand with
powder coated
SPACE REQUIRED : 1.5 m. (L) x 1.0 m(W) X 2.0 m (H)
SERVICE REQUIRED : Air Supply : : @ 6 CFM, at4 Kg /cm2.
CHEMICALS REQUIRED : Tolune , Acetic Acid , Distilled Water
, NaOH , Phenolphthalein , Benzene
WEIGHT : @ 45 Kg

Get More Details:- 25- SINGLE DROP EXTRACTION COLUMN

DIFFUSION COEFFICIENT OF VOLATILE LIQUID IN AIR

DESCRIPTION : The experimental set up consists of glass U tube with a capillary base. The U tube is immersed in water tank. . A scale is provided in front of the capillary for measurement of fall liquid level. Fan is provided to blow a gentle current of air over the capillary box, at a rate controlled by a valve. The tank temperature & in turn the liquid temperature is measured by the thermometer RANGE OF EXPERIMENTS TO BE CARRIED OUT: Study of diffusion of CCL4 in air EXPERIMENTAL SETUP : Stephens Tube : Borosilicate Glass Heater : Magnetic Stirrer with Hot plat Blower : ¼ HP Measuring Scale : 1No. Digital Temp Indicator : 0 – 200 0 C., Sensor : CR/AL Type Piping : SS , PVC Setup Mounting : On sturdy MS stand with powder coated SPACE REQUIRED : 1.0 m. (L) x 1.0 m(W) X 1.0 m (H) SERVICE REQUIRED : Power Supply : 230 V, 50 Hz, A. C. CHEMICALS REQUIRED : CCL4 WEIGHT : @ 45 Kg

Get More Details:- 26- DIFFUSION COEFFICIENT OF VOLATILE LIQUID IN AIR

LIQUID LIQUID DIFFUSION

DESCRIPTION : The experimental set up consists of Porous pot in which solution is filled. The Porous pot is immersed in water Still. A conductivity meter is used to measure the conductivity of water still changes with time.A magnetic stirrer is used to agitate the solution. RANGE OF EXPERIMENTS TO BE CARRIED OUT: Study of diffusion of liquid in liquid EXPERIMENTAL SETUP : Poros Pot : 1 No. Heater : Magnetic Stirrer with Hot plat Conductivity Meter : 1 No Type Piping : SS , PVC Setup Mounting : On sturdy MS stand with powder coated SPACE REQUIRED : 1.0 m. (L) x 1.0 m(W) X 1.0 m (H) SERVICE REQUIRED : Power Supply : 230 V, 50 Hz, A. C. WEIGHT : @ 45 Kg

Get More Details:- 27- LIQUID LIQUID DIFFUSION

DIFFUSION OF SOLID IN AIR

DESCRIPTION : The experimental set up consists of glass tube.. . A Weighing balance is provided for measurement of loss in weight . Fan is provided to blow a gentle current of air over the tube, at a rate controlled by a valve. RANGE OF EXPERIMENTS TO BE CARRIED OUT : Study of diffusion of Solid in Air EXPERIMENTAL SETUP : Air Fan : 1 No Digital Weighing Balance : 1 no Setup Mounting : On sturdy MS stand with powder coated SPACE REQUIRED : 1.0 m. (L) x 1.0 m(W) X 1.0 m (H) SERVICE REQUIRED : Power Supply : 230 V, 50 Hz, A. C. CHEMICALS REQUIRED : CCL4 WEIGHT : @ 45 Kg

Get More Details:- 28-DIFFUSION OF SOLID IN AIR

SOLID DISSOLUTION APPARATUS

DESCRIPTION : In the system solid get transferred into the liquid phase. This transfer result from molecular diffusion as well as eddy diffusion . Because eddy diffusion currents are formed by stirring the system with the help of magnetic stirrer . Due to this concentration of solid in liquid goes on increasing with respect to time .If we provide sufficient time , then this concentration will achieve the value CA which is maximum possible solubility of solid at that temperature.
RANGE OF EXPERIMENTS :
To determine the solid – liquid mass transfer coefficient for given system
EXPERIMENTAL SETUP :
Dissolution Vessel : Borosilicate Glass
Stirrer : SS impeller and shaft coupled to
FHP Motor
Digital Temp Indicator : 0 – 200 0 C ., Indicator cum Controller
Temp Sensor : CR/AL Type
Heater : Nichrome Wire
Setup Mounting : On sturdy MS stand with
powder coated
SPACE REQUIRED : 1 m. (L) x 0.5 m(W) X 1.0 m (H)
SERVICE REQUIRED : Power Supply : 230 V, 50 Hz, A. C.
CHEMICALS REQUIRED : Benzoic Acid
WEIGHT : @ 45 Kg

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ASTM DISTILLATION SETUP

DESCRIPTION : An A.S.T.M. distillation is a simple distillation using The equipment consists of Borosilicate glass round bottom flask as distillation still . The distillation is carried out by heating the still. The vapors coming from the column is going in to the condenser. The distillate is collected in measuring flask. RANGE OF EXPERIMENTS TO BE CARRIED OUT : To A.S.T.M. Distillation EXPERIMENTAL SETUP : Reboiler : Borosilicate glass round bottom flask Distillate Receiver : Borosilicate glass measuring cylinder Condenser : Borosilicate glass double pipe condenser Heating Mantle : Aluminum body with fiber cloth and with Thermostat Digital Temp Indicator : 0 – 400 0 C . Temp Sensor : CR/AL Type Piping : PVC Setup Mounting : On sturdy MS stand with powder coated SPACE REQUIRED : 1.5 m. (L) x 1.0 m(W) X 2 m (H) SERVICE REQUIRED : Power Supply : 230 V, 50 Hz, A. C. CHEMICALS REQUIRED : Methanol Or Ethanol WEIGHT : @ 45 Kg

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