BUBBLE CAP DISTILLATION SETUP

/in /by

DESCRIPTION: The equipment consists of stainless steel column with reboiler. The bubble caps are fitted in the column at proper locations. The distillation is carried out by heating the still. The vapors coming from the column is going in to the condenser. The distillate is collected in the distillate receiver , part of which or complete distillate is recycled as reflux.
RANGE OF EXPERIMENTS TO BE CARRIED OUT :
1. To carryout distillation in Bubble cap column.
2. To calculate the number of trays required
3. To establish the overall tray efficiency of the distillation
4. To study the practical significance of McCabe – Thiele method.
EXPERIMENTAL SETUP :
Reboiler : Material Stainless Steel
Column : Material Stainless Steel
Reflux Drum : Material Stainless Steel.
Condenser : SS , Shell and Tube type Condenser
Packing : Bubble Cap ,
Heating Mantle : Aluminum body with fiber cloth
Digital Temp Indicator : 0 – 400 0 C ,
Temp Sensor : CR/AL Type
Distillate Receiver : Material Stainless Steel
Piping : SS , PVC
Setup Mounting : On sturdy MS stand with
powder coated
SPACE REQUIRED : 1.5 m. ( L) x 1.0 m (W) X 3.0 m (H).
SERVICE REQUIRED: Power Supply : 230 V, 50 Hz, A.C.
Water Supply : @ 2 lpm
Specific Gravity Bottle
CHEMICALS REQUIRED : Methanol Or Ethanol ,
WEIGHT : @ 85 Kg

Get More Details:- 11-BUBBLE CAP COLUMN DISTILLATION SETUP

SIEVE TRAY DISTILLATION SETUP

/in /by

DESCRIPTION: The equipment consists of stainless steel column with reboiler. The Sieve trays are fitted in the column at proper locations still. The distillation is carried out by heating the still. The vapors coming from the column is going in to the condenser. The distillate is collected in the distillate receiver
RANGE OF EXPERIMENTS TO BE CARRIED OUT :
1. To carryout distillation in Sieve plate distillation.
2. To calculate the number of trays required
3. To establish the overall tray efficiency of the distillation
4. To study the practical significance of McCabe – Thiele method.
EXPERIMENTAL SETUP :
Reboiler : Material Stainless Steel
Column : Material Stainless Steel
Condenser : SS , Shell and Tube type Condenser
Reflux Drum : Material Stainless Steel.
Packing : Sieve Trays .
Heating Mantle : Aluminum body with fiber cloth
Digital Temp Indicator : 0 – 400 0 C .
Temp Sensor : CR/AL Type
Distillate Receiver : Material Stainless Steel
Piping : SS , PVC
Setup Mounting : On sturdy MS stand with
powder coated
SPACE REQUIRED : 1.5 m. ( L) x 1.0 m (W) X 3.0m (H).
SERVICE REQUIRED : Power Supply : 230 V, 50 Hz, A.C.
Water Supply : @ 2 lpm
Specific Gravity Bottle
CHEMICALS REQUIRED : Methanol Or Ethanol .
WEIGHT : @ 85 Kg

Get More Details:- 12-SIEVE TRAY COLUMN DISTILLATION SETUP

PACKED COLUMN DISTILLATION SETUP

/in /by

DESCRIPTION: The equipment consists of stainless steel column with reboiler. The Raschig Rig Packing are fitted in the column at proper locations still. The distillation is carried out by heating the still. The vapors coming from the column is going in to the condenser. The distillate is collected in the distillate receiver
RANGE OF EXPERIMENTS TO BE CARRIED OUT :
1. To carryout distillation in Sieve plate distillation.
2. To calculate the number of trays required
3. To establish the overall tray efficiency of the distillation
4. To study the practical significance of McCabe – Thiele method.
EXPERIMENTAL SETUP :
Reboiler : Material Stainless Steel
Column : Material Stainless Steel
Packing : Raschig Rig
Condenser : SS , Shell and Tube type Condenser
Reflux Drum : Material Stainless Steel.
Packing : Sieve Trays .
Heating Mantle : Aluminum body with fiber cloth
Digital Temp Indicator : 0 – 400 0 C .
Temp Sensor : CR/AL Type
Distillate Receiver : Material Stainless Steel
Piping : SS , PVC
Setup Mounting : On sturdy MS stand with
powder coated
SPACE REQUIRED : 1.5 m. ( L) x 1.0 m (W) X 3.0m (H).
SERVICE REQUIRED : Power Supply : 230 V, 50 Hz, A.C.
Water Supply : @ 2 lpm
Specific Gravity Bottle
CHEMICALS REQUIRED : Methanol Or Ethanol .
WEIGHT : @ 85 Kg

Get More Details:- 13-PACKED COLUMN DISTILLATION SETUP

FRACTIONAL DISTILLATION SETUP

/in /by

DESCRIPTION: The equipment consists of Borosilicate Glass column with reboiler. The Raschig Rig Packing are fitted in the column at proper locations still. The distillation is carried out by heating the still. The vapors coming from the column is going in to the condenser. The distillate is collected in the distillate receiver
RANGE OF EXPERIMENTS TO BE CARRIED OUT:
1. To carryout Fractional distillation.
EXPERIMENTAL SETUP :
Reboiler : Borosilicate glass
Column : Borosilicate glass
Condenser : Borosilicate glass
Packing : Rascig rings
Heating Mantle : Aluminum body with fiber cloth
Digital Temp Indicator : 0 – 400 0 C .
Temp Sensor : CR/AL Type
Distillate Receiver : Borosilicate glass
Piping : SS , PVC
Setup Mounting : On sturdy MS stand with
powder coated
SPACE REQUIRED : 1.5 m. (L) x 1.0 m(W) X 3 m (H)
SERVICE REQUIRED : Power Supply : 230 V, 50 Hz, A.C.
Water Supply : @ 2 lpm
Specific Gravity Bottle
CHEMICALS REQUIRED : Methanol Or Ethanol ,
Specific Gravity Bottle
WEIGHT : @ 65 Kg

Get More Details:- 14-FRACTIONAL DISTILLATION SETUP

BATCH DISTILLATION SETUP

/in /by

DESCRIPTION: The equipment consists of Borosilicate Glass column with reboiler. The Raschig Rig Packing are fitted in the column at proper locations still. The distillation is carried out by heating the still. The vapors coming from the column is going in to the condenser. The distillate is collected in the distillate receiver
RANGE OF EXPERIMENTS TO BE CARRIED OUT:
1. To carryout Batch distillation.
EXPERIMENTAL SETUP :
Reboiler : Borosilicate glass
Column : Borosilicate glass
Condenser : Borosilicate glass
Packing : Rascig rings
Heating Mantle : Aluminum body with fiber cloth
Digital Temp Indicator : 0 – 400 0 C .
Temp Sensor : CR/AL Type
Distillate Receiver : Borosilicate glass
Piping : SS , PVC
Reflux Divider : Magnetically Opearated
Setup Mounting : On sturdy MS stand with
powder coated
SPACE REQUIRED : 1.5 m. (L) x 1.0 m(W) X 3 m (H)
SERVICE REQUIRED : Power Supply : 230 V, 50 Hz, A.C.
Water Supply : @ 2 lpm
Specific Gravity Bottle
CHEMICALS REQUIRED : Methanol Or Ethanol ,
Specific Gravity Bottle
WEIGHT : @ 65 Kg

Get More Details:- 15-BATCH DISTILLATION SETUP

DISTILLATION AT TOTAL REFLUX

/in /by

DESCRIPTION: The equipment consists of Borosilicate Glass column with reboiler. The Raschig Rig Packing are fitted in the column at proper locations still. The distillation is carried out by heating the still. The vapors coming from the column is going in to the condenser. The distillate is collected in the distillate receiver
RANGE OF EXPERIMENTS TO BE CARRIED OUT:
1. To carryout distillation at total reflux.
EXPERIMENTAL SETUP :
Reboiler : Borosilicate glass
Column : Borosilicate glass
Condenser : Borosilicate glass
Packing : Rascig rings
Heating Mantle : Aluminum body with fiber cloth
Digital Temp Indicator : 0 – 400 0 C .
Temp Sensor : CR/AL Type
Distillate Receiver : Borosilicate glass
Piping : SS , PVC
Reflux Divider : Magnetically Opearated
Setup Mounting : On sturdy MS stand with
powder coated
SPACE REQUIRED : 1.5 m. (L) x 1.0 m(W) X 3 m (H)
SERVICE REQUIRED : Power Supply : 230 V, 50 Hz, A.C.
Water Supply : @ 2 lpm
Specific Gravity Bottle
CHEMICALS REQUIRED : Methanol Or Ethanol ,
Specific Gravity Bottle
WEIGHT : @ 65 Kg

Get More Details:- 16- DISTILLATION AT TOTAL REFLUX

FRACTIONAL REACTION DISTILLATION

/in /by

DESCRIPTION: The unit consists of a packed column with rasching rings. Two necked round bottom borosilicate glass flask with a heating metal is used as a reboiler. The vapor stream flows up the column & is condensed in the condenser.
RANGE OF EXPERIMENTS TO BE CARRIED OUT :
To carryout Fractional reaction distillation
EXPERIMENTAL SETUP :
Reboiler : Borosillicate Glass
Column : Borosillicate Glass
Stirrer : SS impeller and shaft coupled to
: FHP Motor
Condenser : Coil type Borosilicate glass.
Packing : Rasching Ring.
Heating Mantle : Aluminum body with fiber cloth
Digital Temp Indicator : 0 – 400 0 C.
Temp Sensor : CR/AL Type
Distillate Receiver : Borosillicate Glass
Piping : SS , PVC
Setup Mounting : On sturdy MS stand with
powder coated
SPACE REQUIRED : mtr. Length x 1.0 mtr. Width X 3 m
SERVICE REQUIRED: Power Supply : 230 V, 50 Hz, A.C.
Water Supply : @ 2 lpm
Specific Gravity Bottle
CHEMICALS REQUIRED : Methanol Or Ethanol
WEIGHT : @ 65 Kg

Get More Details:- 17- FRACTIONAL REACTION DISTILLATION

VACUUM DISTILLATION SETUP

/in /by

DESCRIPTION : The experimental set up consists of a distillation still. The distillation steel is surrounded by another still is constructed of mild steel. The vapour coming from the steel are sucked by means of vaccum pump. only non condensable gases go to the pump while the vapours are condensed by the water called condenser. Water is circulated through the condenser tube . The bottom product from the steel is discharged by means of the bottom drain point while the condensed vapour is discharge by means of the drain. RANGE OF EXPERIMENTS : 1. To carryout distillation under vaccum. 2. To Verify Rayleigh equation. EXPERIMENTAL SETUP : Reboiler : Material Stainless Steel Column : Material Stainless Steel Reflux Drum : Material Stainless Steel Condenser : SS , Shell and Tube type Condenser Flow Measurement : 1 No. Pre calibrated Rota meter Packing : Rasching Ring. Heating Mantle : Aluminum body with fiber cloth Digital Temp Indicator : 0 – 400 0 C. Temp Sensor : CR/AL Type Distillate Receiver : Material Stainless Steel Vacuum Pump : Compactable capacity Piping : SS , PVC Setup Mounting : On sturdy MS stand with powder coated SPACE REQUIRED : 1.5 m. (L) x 1.0 m(W) X 2.0 m (H) SERVICE REQUIRED: Power Supply : 230 V, 50 Hz, A.C. Water Supply : @ 2 lpm Specific Gravity Bottle CHEMICALS REQUIRED : Methanol Or Ethanol WEIGHT : @ 65 Kg.

Get More Details:- 18- VACUUM DISTILLATION SETUP

EQUILLIBRIUM FLASH DISTILLATION SETUP

/in /by

DESCRIPTION : The apparatus consists of an overhead tank which contains liquid undergoing distillation. The liquid from the tank is metered through the Rota meter & then goes inside the copper coil in the boiler. Steam condenses outside the coil. The liquid then enters the flash chamber after being throttled by a valve. In the flash chamber the liquid flashes into vapors partially. The vapors are left to the condenser where they are condensed by water. Condensed vapors are collected & quantity measured. The enriched liquid at the bottom of the chamber is collected & measured.
RANGE OF EXPERIMENTS TO BE CARRIED OUT :
To study equilibrium flash distillation .

EXPERIMENTAL SETUP :
Reboiler : Material Stainless Steel
Column : Material Stainless Steel
Condenser : SS , Shell and Tube type Condenser
Flow Measurement : 2 No. Pre calibrated Rota meter
Flash Chamber : Material Stainless Steel.
Steam Generator : Electrically heated with
Pressure Gauge, Safety Valve
Digital Temp Indicator : 0 – 400 0 C .
Temp Sensor : CR/AL Type
Distillate Receiver : Material Stainless Steel
Piping : SS , PVC
Setup Mounting : On sturdy MS stand with
powder coated
SPACE REQUIRED : 1.5 m. (L) x 1.0 m(W) X 3 m (H)
SERVICE REQUIRED : Power Supply : 440 V, 50 Hz, A.C.
Water Supply : @ 2 lpm b
Specific Gravity Bottle
CHEMICALS REQUIRED : Methanol Or Ethanol
WEIGHT : @ 65 Kg

Get More Details:- 19- EQUILLIBRIUM FLASH DISTILLATION

SOLID LIQUID EXTRACTION ( LEACHING )

/in /by

DESCRIPTION : This setup is designed to study the performance characteristics of solvent extraction of particular component from packed bed of solid material . The apparatus allows study of such systems as water / inorganic salts , water /sugar bed , Methylene chloride / vegetable oil etc.The glass column fitted Teflon mesh to support the solid material. The
solvent is introduced near the bottom of column and it flow upward counter- currently to solids.
RANGE OF EXPERIMENTS TO BE CARRIED OUT :
To study various systems parameters like , solvent temperature,
solvent rate and particle on the % recovery of oil from solid.
To determine the volume mass transfer coefficient in solid
l iquid extraction
EXPERIMENTAL SETUP
Column : Stainless steel column
Condenser : Shell and tube condenser SS
Solvent Receiver : Stainless steel
Heating Mantle : Aluminum body with fiber cloth
Piping : SS , PVC
Setup Mounting : On sturdy MS stand with
powder coated
SPACE REQUIRED : 1.5 m. (L) x 1.0 m(W) X 1.5 m (H)
SERVICE REQUIRED : Power Supply : 230 V, 50 Hz, A.C.
Water Supply : @ 6 CFM, at 4 kg/cm2
CHEMICALS REQUIRED : Hexane, Ground nut
WEIGHT : @ 65 Kg

Get More Details:- 20- SOLID LIQUID EXTRACTION LEACHING